N-[(1,1-二甲基乙氧基)羰基]-L-异亮氨酸甲酯合成路线 （共 18 条）
反应条件
triethylamine in dichloromethane T=25°C; 12 h; Inert atmosphere;
参考文献
Yang, Dezhi; Wang, Peng; Liu, Jianzhen; Xing, Hualu; Liu, Yang; Xie, Wencheng; Zhao, Guisen
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 1 p. 366 - 373
反应条件
potassium hydrogencarbonate in dimethyl sulfoxide T=90°C; 18 h; Inert atmosphereGreen chemistry;
参考文献
Ji, Yuan; Sweeney, Jessica; Zoglio, Jillian; Gorin, David J.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11606 - 11611
反应条件
in methanol; diethyl ether T=4°C; Methylation;
参考文献
Lin; Chen; You; Chen Liu; Lee
Journal of Natural Products, 2000 , vol. 63, # 10 p. 1338 - 1343
反应条件
potassium fluoride; triethylamine in N,N-dimethyl-formamide 5 h; Ambient temperature;
参考文献
Li, Wen-Ren; Jiang, Jianjun; Joullie, Madelaine M.
Tetrahedron Letters, 1993 , vol. 34, # 9 p. 1413 - 1414
反应条件
in acetonitrile T=20°C;
参考文献
Sameiro, M; Goncalves, T; Maia, Hernani L.S
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7775 - 7777
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Sameiro; Goncalves; Maia, Hernani L.S.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1480 - 1485
参考文献
Van den Broek; Fennis; Arevalo; Lazaro; Ballesta; Lelieveld; Ottenheijm
European Journal of Medicinal Chemistry, 1989 , vol. 24, # 5 p. 503 - 510
反应条件
potassium hydrogencarbonate in N,N-dimethyl-formamide Ambient temperature;
参考文献
Hamada, Yasumasa; Shibata, Makoto; Sugiura, Tsuneyuki; Kato, Shinji; Shioiri, Takayuki
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1252 - 1255
反应条件
1: 56 percent / DMAP / acetonitrile / 20 °C 2: 72 percent / acetonitrile / 20 °C View Scheme
参考文献
Sameiro, M; Goncalves, T; Maia, Hernani L.S
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7775 - 7777
反应条件
1: 56 percent / DMAP / acetonitrile / 20 °C 2: 72 percent / acetonitrile / 20 °C View Scheme
参考文献
Sameiro; Goncalves; Maia, Hernani L.S.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1480 - 1485
反应条件
1: 79 percent / DCC; HOBt / dimethylformamide 2: 56 percent / DMAP / acetonitrile / 20 °C 3: 72 percent / acetonitrile / 20 °C View Scheme
参考文献
Sameiro; Goncalves; Maia, Hernani L.S.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1480 - 1485
