三甲基-(4-甲基苯氧基)硅烷合成路线 (共 16 条)
反应条件
n-butyllithium 1.) ether, room temp., 0.33 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
sodium 1.) dioxane/ether, RT, overnight, 2.) dioxane/ether, RT, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Heinicke, Joachim; Kadyrov, Renat
Journal of Organometallic Chemistry, 1996 , vol. 520, # 1-2 p. 131 - 137
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Tietze, Lutz-F.; Fischer, Roland; Guder, Hans-Joachim
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4661 - 4664
反应条件
[Ru(II)(2,2’-bipyridine)3]Cl2; carbon tetrabromide in acetonitrile T=20°C; Irradiation;
参考文献
Zhao, Yating; Li, Zhe; Yang, Chao; Lin, Run; Xia, Wujiong
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 622 - 627
反应条件
[bis(acetoxy)iodo]benzene in water; acetonitrile
T=0 - 20°C; 3 h;
参考文献
Felpin, Francois-Xavier
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 409 - 412
反应条件
in benzonitrile
T=36°C; Rate constant;
参考文献
Kozuka, Seizi; Higashino, Tetsuji
Tetrahedron Letters, 1980 , vol. 21, p. 2067 - 2068