4-(1-甲基-1H-4-吡唑)苯甲醛合成路线 (共 4 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in ethylene glycol dimethyl ether; water T=90°C; Suzuki Coupling; 0.0833333 h; Microwave irradiationInert atmosphere;
参考文献
Cheng, Hua; Wu, Qiong-You; Han, Fan; Yang, Guang-Fu
Chinese Chemical Letters, 2014 , vol. 25, # 5 p. 705 - 709
反应条件
tetrakis(triphenylphosphine) palladium(0) in xylene T=140°C; 3 h;
参考文献
Tanaka, Akira; Terasawa, Takeshi; Hagihara, Hiroyuki; Sakuma, Yuri; Ishibe, Noriko; Sawada, Masae; Takasugi, Hisashi; Tanaka, Hirokazu
Journal of Medicinal Chemistry, 1998 , vol. 41, # 13 p. 2390 - 2410
反应条件
PdCl(C3H5)(dppb); potassium acetate in N,N-dimethyl-formamide T=150°C; 72 h; Inert atmosphere; Reagent/catalyst; Overall yield = 38 percent;
参考文献
Takfaoui, Abdelilah; Zhao, Liqin; Touzani, Rachid; Dixneuf, Pierre H.; Doucet, Henri
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1697 - 1701
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Beladhria, Anissa; Beydoun, Kassem; Ammar, Hamed Ben; Salem, Ridha Ben; Doucet, Henri
Synthesis, 2011 , # 16 art. no. C22411SS, p. 2553 - 2560