顺 -1,2-环己二醇合成路线 （共 184 条）
反应条件
C42H60N6O7 in toluene T=-20°C; 4.5 h; Reagent/catalystTime;
参考文献
Mueller, Christian E.; Zell, Daniela; Hrdina, Radim; Wende, Raffael C.; Wanka, Lukas; Schuler, Soeren M. M.; Schreiner, Peter R.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8465 - 8484
反应条件
in chloroform-d1 T=20°C; 5.75 h; Title compound not separated from byproducts.;
参考文献
Roy, Chandra D.; Brown, Herbert C.
Monatshefte fur Chemie, 2007 , vol. 138, # 9 p. 879 - 887
反应条件
dihydrogen peroxide; TAPO-5 in water T=80°C; 24 h; Further byproducts given;
参考文献
Lee, Sang-Ok; Raja, Robert; Harris, Kenneth D. M.; Thomas, John Meurig; Johnson, Brian F. G.; Sankar, Gopinathan
Angewandte Chemie - International Edition, 2003 , vol. 42, # 13 p. 1520 - 1523
反应条件
1: diethyl ether; sulfuric acid 2: pyridine 3: acetic acid anhydride; glacial acetic acid View Scheme
参考文献
Winstein et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 816,818
反应条件
hydrogenchloride; sodium tungstate; phosphoric acid; dihydrogen peroxide T=90°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 51, # 9 p. 1599 - 1602
反应条件
dihydrogen peroxide; TAPO-5 in water T=80°C; 24 h; Further byproducts given;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 13 p. 1520 - 1523
反应条件
1: With para-iodobenzoic acid in water-d2; acetonitrile-D3 T=60°C; 0.166667 h; 2: With potassium peroxymonosulfate in water-d2; acetonitrile-D3 T=60°C;
参考文献
Organic Letters, , vol. 12, # 24 p. 5640 - 5643
反应条件
1: With para-iodobenzoic acid in water-d2; acetonitrile-D3 T=60°C; 0.166667 h; 2: With potassium peroxymonosulfate in water-d2; acetonitrile-D3 T=60°C;
参考文献
Organic Letters, , vol. 12, # 24 p. 5640 - 5643
反应条件
formic acid T=20 - 240°C; Inert atmosphere;
参考文献
Chemical Communications, , # 23 p. 3357 - 3359
反应条件
dimethyl sulfoxide; trifluoroacetic anhydride in dichloromethane
T=-60°C; 1.5 h;
参考文献
Amon, Catherine M.; Banwell, Martin G.; Gravatt, G.Lance
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 4851 - 4855
