顺 -1,2-环己二醇合成路线 （共 184 条）
反应条件
sulfuric acid Electrolysis;
参考文献
Yakugaku Zasshi, , vol. 56, p. 455
Chem.Abstr., , p. 165
反应条件
water; NAF 1.) hexane, 25 grad C, Ar atmosphere, 1 h, 2.) methylenechloride, 25 grad C, 0.5 h.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 23, # 35 p. 3597 - 3600
反应条件
acetic acid; platinum Hydrogenation;
参考文献
Nippon Kagaku Kaishi, , vol. 64, p. 972,974
Chem.Abstr., , p. 3803
反应条件
potassium hydroxide; potassium acetate; acetic acid 1.) reflux, 16 h, 2.) CH3OH, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Acta Chemica Scandinavica, , vol. 43, # 9 p. 902 - 907
反应条件
1: 1) 1.5 M nBuLi, 2) I2 / 1) THF, hexane, r.t., 2) THF, hexane, r.t. 2: 1) Bu3SnH, 2) base View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 10 p. 465 - 466
反应条件
1: KHSO4 / 150 - 160 °C 2: lead (IV)-acetate; glacial acetic acid / 25 - 45 °C / Behandlung des Reaktionsprodukts mit wss. NaOH oder aethanol. KOH 3: ethanol; platinum / Hydrogenation View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 481, p. 263,286
Chemische Berichte, , vol. 64, p. 260,264
反应条件
1: water / 90 - 95 °C 2: ethanol; platinum / Hydrogenation View Scheme
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 204, p. 1350
反应条件
1: lead (IV)-acetate; glacial acetic acid / 25 - 45 °C / Behandlung des Reaktionsprodukts mit wss. NaOH oder aethanol. KOH 2: ethanol; platinum / Hydrogenation View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 481, p. 263,286
Chemische Berichte, , vol. 64, p. 260,264
反应条件
lithium aluminium tetrahydride; dihydrogen peroxide; trifluoroacetic anhydride 1.) CH2Cl2, 20 deg C, 3 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 822 - 827
反应条件
lithium aluminium tetrahydride; oxygen 1.) 60 deg C,101.3 kPa; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 322, # 6 p. 915 - 932
