4,4'-(2,5-二丁氧基-1,4-亚苯基)二(2-甲基-3-丁炔-2-醇)合成路线 (共 3 条)
反应条件
copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride T=70°C; 18 h;
参考文献
Pelter, Andrew; Jones, D. Elfyn
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 14 p. 2289 - 2294
反应条件
1: 80 percent / Br2 / CCl4 / 70 h / Heating 2: 86 percent / Pd(PPh3)4; nPrNH2 / 70 h / 65 °C View Scheme
参考文献
Ziessel, Raymond; Diring, Stephane; Retailleau, Pascal
Dalton Transactions, 2006 , # 27 p. 3285 - 3290
反应条件
1: 75 percent / NaOH / dimethylformamide / 18 h / 150 °C 2: 80 percent / Br2 / CCl4 / 70 h / Heating 3: 86 percent / Pd(PPh3)4; nPrNH2 / 70 h / 65 °C View Scheme
参考文献
Ziessel, Raymond; Diring, Stephane; Retailleau, Pascal
Dalton Transactions, 2006 , # 27 p. 3285 - 3290