1,1,3,3,5,5-五甲基二乙氧基三硅烷合成路线 （共 5 条）
反应条件
NaOH in sodium hydroxide aq. NaOH; addn. of 40.7 mol H2O and about 0.5 mol NaOH to 54.4 mol (CH3)2Si(OC2H5)2; heating at 70-100°C; further products;;
参考文献
Gmelin Handbook: Si: MVol.C, 105, page 289 - 291
反应条件
NaOH in sodium hydroxide aq. NaOH; addn. of 40.7 mol H2O and about 0.5 mol NaOH to 54.4 mol (CH3)2Si(OC2H5)2; heating at 70-100°C; further products;;
参考文献
Gmelin Handbook: Si: MVol.C, 105, page 289 - 291
反应条件
NaOH in sodium hydroxide aq. NaOH; addn. of 40.7 mol H2O and about 0.5 mol NaOH to 54.4 mol (CH3)2Si(OC2H5)2; heating at 70-100°C; further products;;
参考文献
Gmelin Handbook: Si: MVol.C, 105, page 289 - 291
反应条件
sodium hydroxide; water weitere Nebenprodukte: Verbindungen C2H5OSi(CH3)2O<Si(CH3)2O>nSiCH3)2OC2H5 (n = 2 bis 9);
参考文献
Dow Chem.Co.
Patent: US2415389 , 1944 ;
Full Text Show Details
Fletcher; Hunter
Journal of the American Chemical Society, 1949 , vol. 71, p. 2922
反应条件
toluene-4-sulfonic acid in n-heptane T=20 - 30°C; 0.5 h; other 2-ethoxy-1,3-dioxanes, other reagents; Product distribution;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1989 , vol. 304, # 1-6 p. 49 - 50
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 304, # 4 p. 883 - 885
