2-(4-氰基苯基)苯并噻唑合成路线 (共 21 条)
反应条件
Na2S2O5 in dimethyl sulfoxide T=120°C; 1 h; Microwave irradiation;
参考文献
Shelkar, Radheshyam; Sarode, Sachin; Nagarkar, Jayashree
Tetrahedron Letters, 2013 , vol. 54, # 51 p. 6986 - 6990
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate T=100°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Wen, Xiaoan; Bakali, Jamal El; Deprez-Poulain, Rebecca; Deprez, Benoit
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2440 - 2443
反应条件
1-methyl-pyrrolidin-2-one T=100°C; 1 h;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
反应条件
potassium phosphate; copper(l) iodide; triphenylphosphine in dimethyl sulfoxide T=160°C; 8 h;
参考文献
Yoshizumi, Tomoki; Tsurugi, Hayato; Satoh, Tetsuya; Miura, Masahiro
Tetrahedron Letters, 2008 , vol. 49, # 10 p. 1598 - 1600
反应条件
palladium diacetate T=60 - 75°C; 12 h; Ionic liquid;
参考文献
Kalkhambkar, Rajesh G.; Laali, Kenneth K.
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4212 - 4215
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
copper diacetate; triethylamine in ethanol T=70°C; 6 h;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Wu, Xia
Organic Letters, 2013 , vol. 15, # 7 p. 1598 - 1601
反应条件
1: 2-(methylthio)benzothiazole With 3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile T=35°C; 2: para-bromobenzonitrile With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide; acetonitrile T=35°C; Barbier type reaction;
参考文献
Begouin, Jeanne-Marie; Rivard, Michael; Gosmini, Corinne
Chemical Communications, 2010 , vol. 46, # 32 p. 5972 - 5974
反应条件
1: 2-(methylthio)benzothiazole With 3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile T=35°C; 2: para-iodobenzonitrile With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide; acetonitrile T=35°C; Barbier type reaction;
参考文献
Begouin, Jeanne-Marie; Rivard, Michael; Gosmini, Corinne
Chemical Communications, 2010 , vol. 46, # 32 p. 5972 - 5974
反应条件
1,10-phenanthroline; niobium bromide; lithium tert-butylate in diethylene glycol dimethyl ether T=150°C; 4 h;
参考文献
Hachiya, Hitoshi; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2009 , vol. 11, # 8 p. 1737 - 1740