反应条件
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -78°C, slow warming to room temp., stirring (25°C, 12 h); removement of solvent (25°C, 12 Torr), removement of Me3SnBr by fractional distillation (30°C, 1E-2 Torr or 53-55°C, 12 Torr); elem. anal.;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
