反应条件
in benzene
1 equiv of the acetylene adding to a susp. 2 equiv of K-graphite in C6H6 under dry N2, 0.5 equiv of borane adding dropwise, stirring for 3 d atroom temp., solids removing by centrifugation, volatiles removing by freezing in vacuo; not isolated, identified by mass spectrum;
参考文献
Kerk, Sies M. van der; Budzelaar, Peter H. M.; Hoof, Anca van der Kerk-van; Kerk, Gerrit J. M. van der; Schleyer, Paul von Rague
Angewandte Chemie, 1983 , vol. 95, p. 61 - 61
