1-(4-甲基苯基)-2,2,2-三氯乙醇合成路线 (共 24 条)
反应条件
potassium hydroxide in methanol; N,N-dimethyl-formamide T=-10°C; 1 h;
参考文献
Mellin-Morliere, Christelle; Aitken, David J.; Bull, Steven D.; Davies, Stephen G.; Husson, Henri-Philippe
Tetrahedron Asymmetry, 2001 , vol. 12, # 1 p. 149 - 155
反应条件
aluminium trichloride T=-10 - 0°C; 12 h;
参考文献
Menegheli, Paulo; Rezende, Marcos Caroli; Zucco, Cezar
Synthetic Communications, 1987 , vol. 17, # 4 p. 457 - 464
反应条件
tetraethylammonium p-toluenesulfonate in chloroform; N,N-dimethyl-formamide cathodic anion chain reaction in a cell equipped with carbon rod electrodes and a ceramic diaphragm;
参考文献
Shono, Tatsuya; Ohmizu, Hiroshi; Kawakami, Souta; Nakano, Shinji; Kise, Naoki
Tetrahedron Letters, 1981 , vol. 22, p. 871 - 874
反应条件
1: para-bromotoluene With magnesium in diethyl ether 2: chloral in diethyl ether 1 h; Heating;
参考文献
Himbert, Gerhard; Gerulat, Oliver
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2001 , vol. 56, # 11 p. 1196 - 1204
反应条件
potassium hydroxide; chloroform
参考文献
Bergmann et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 5012
参考文献
Beasley, Helen L.; Phongkham, Thipsavanh; Daunt, Margaret H.; Guihot, Simone L.; Skerritt, John H.
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 8 p. 3339 - 3352
参考文献
Chattaway; Muir
Journal of the Chemical Society, 1934 , p. 701
参考文献
Jozitsch
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1902 , vol. 34, p. 101
Bulletin de la Societe Chimique de France, 1902 , vol. <3> 28, p. 923
反应条件
1,3,5-Trinitrobenzene T=25°C; determination of rate of formation; var. trihalogeno acetic acid;;
参考文献
Atkins, Paul J.; Gold, Victor; Wassef, Wasfy N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1247 - 1252
反应条件
Further byproducts given;
参考文献
Reeve, Wilkins; McKee, James R.; Brown, Robert; Lakshmanan, Sitarama; McKee, Gertrude A.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 485 - 493