1,4-双[(三甲基硅基)乙炔基]苯合成路线 （共 20 条）
反应条件
Sonogashira cross-coupling;
参考文献
Chemical Communications, , # 13 p. 1430 - 1432
反应条件
copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride T=70°C; 3.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 14 p. 2289 - 2294
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=20°C; Hagihara-Sonogashira coupling; 18 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 5 p. 946 - 953
反应条件
n-Bu2CuLi in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
European Journal of Organic Chemistry, , # 4 p. 660 - 665
反应条件
zinc in acetonitrile T=120°C; 5 h; in a sealed tube;
参考文献
Tetrahedron Letters, , vol. 36, # 16 p. 2769 - 2772
反应条件
[{Ir(l-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine in toluene T=80°C; 24 h; Inert atmosphere;
参考文献
Organometallics, , vol. 30, # 9 p. 2539 - 2545
反应条件
tin(ll) chloride in ethanol; water; acetic acid T=60°C; 0.166667 h;
参考文献
New Journal of Chemistry, , vol. 29, # 7 p. 972 - 976
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 2 h; Heating;
参考文献
Synthesis, , # 3 art. no. Z14204SS, p. 485 - 492
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate Sonogashira coupling; 17 h; Neat (no solvent);
参考文献
Green Chemistry, , vol. 11, # 11 p. 1821 - 1825
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 2 h; Heating;
参考文献
Synthesis, , # 3 art. no. Z14204SS, p. 485 - 492
