in toluene
soln. of Me2Si(tBuN)2Sn added dropwise to a soln. of the silylamine in toluene, stirring for two hours, refluxing for one hour, volatile substances removed in vacuum and the seconocubane-like intermediate pyrolysed in vacuo at 0.01 Torr and 250°C; product sublimed, elem. anal.;
参考文献
Veith, Michael; Opsoelder, Michael; Zimmer, Michael; Huch, Volker
European Journal of Inorganic Chemistry, 2000 , # 6 p. 1143 - 1146
in toluene
soln. of Me2Si(NtBu)2Sn added dropwise to a soln. of the silylamine in toluene, stirring for two hours, refluxed for one hour, volatile substances removed in vacuum, seconorcubane-like intermediate pyrolysed in vacuo at 0.01 Torr and 250°C; product sublimed, elem. anal.;
参考文献
Veith, Michael; Opsoelder, Michael; Zimmer, Michael; Huch, Volker
European Journal of Inorganic Chemistry, 2000 , # 6 p. 1143 - 1146
