1,2-乙炔二基二(三乙基硅烷)合成路线 （共 9 条）
反应条件
dihydrogen hexachloroplatinate; iodine in hexane T=20°C; 2 h;
参考文献
Voronkov, M. G.; Pukhnarevich, V. B.; Ushakova, N. I.; Tsykhanskaya, I. I.; Albanov, A. I.; Vitkovskii, V. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 94 - 100,80 - 85
反应条件
dihydrogen hexachloroplatinate; iodine in tetrahydrofuran T=20°C; 2 h; Yield given. Title compound not separated from byproducts;
参考文献
Voronkov, M.G.; Ushakova, N.I.; Tsykhanskaya, I.I.; Pukhnarevich, V.B.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 39 - 48
反应条件
dihydrogen hexachloroplatinate; iodine in hexane T=20°C; 2 h;
参考文献
Voronkov, M. G.; Pukhnarevich, V. B.; Ushakova, N. I.; Tsykhanskaya, I. I.; Albanov, A. I.; Vitkovskii, V. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 94 - 100,80 - 85
反应条件
lithium in tetrahydrofuran
参考文献
West,R.; Quass,L.C.
Journal of Organometallic Chemistry, 1969 , vol. 18, p. 55 - 67
反应条件
lithium in tetrahydrofuran
参考文献
West,R.; Quass,L.C.
Journal of Organometallic Chemistry, 1969 , vol. 18, p. 55 - 67
参考文献
Petrov, A. D.; Shchukovskaja, L. L.
Doklady Akademii Nauk SSSR, 1952 , vol. 86, p. 551 - 553
C. A., 1953 , p. 12225
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 31, page 96 - 99
反应条件
magnesium 1.) THF, from reflux temp. to 25 deg C, 1 h, 2.) overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Soderquist, John A.; Rivera, Isaac; Negron, Alvin
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4051 - 4055
参考文献
Petrow; Schtschukowskaja
Doklady Akademii Nauk SSSR, 1952 , vol. 86, p. 551
Chem.Abstr., 1953 , p. 12225
反应条件
H2 in not given hydrogenation (Raney-Ni);;
参考文献
Petrov, A. D.; Shchukovskaja, L. L.
Doklady Akademii Nauk SSSR, 1952 , vol. 86, p. 551 - 553
C. A., 1953 , p. 12225
Full Text Show Details
Topchiev, A. V.; Nametkin, N. S.; Shcherbakova, A. A.
Doklady Akademii Nauk SSSR, 1952 , vol. 86, p. 559 - 560
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 31, page 96 - 99
