6-甲氧基-2,3,4,9-四氢-1H-beta-咔啉-1-酮合成路线 （共 9 条）
反应条件
1: With triethylamine in toluene T=50 - 70°C; 0.416667 h; Inert atmosphere; 2: With hydrogen bromide in acetic acid; toluene 0.5 h; Inert atmosphereReflux;
参考文献
Nicolaou; Kiappes; Tian, Weiwei; Gondi, Vijaya B.; Becker, Jochen
Organic Letters, 2011 , vol. 13, # 15 p. 3924 - 3927
反应条件
formic acid 1 h; Heating;
参考文献
Guengoer, Timur; Malabre, Patrice; Teulon, Jean-Marie; Camborde, Francoise; Meignen, Joelle; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 25 p. 4307 - 4316
反应条件
1: sodium nitrite, 3 M hydrochloric acid 2: 55 percent / H2O / 5 h / 0 °C 3: 58 percent / formic acid / 0.5 h / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 10 p. 849 - 860
反应条件
hydrogenchloride; acetic acid
参考文献
Chemische Berichte, , vol. 90, p. 1060,1067
反应条件
1: 55 percent / H2O / 5 h / 0 °C 2: 58 percent / formic acid / 0.5 h / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 10 p. 849 - 860
反应条件
1: aq.-ethanolic KOH 2: aqueous HCl View Scheme
参考文献
Journal of the Chemical Society, , p. 4589,4591
反应条件
1: 100 percent / KOH / ethanol / 6 h / Heating 2: 72 percent / 10percent aq. HCl / 2 h / Heating View Scheme
参考文献
Guengoer, Timur; Malabre, Patrice; Teulon, Jean-Marie; Camborde, Francoise; Meignen, Joelle; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 25 p. 4307 - 4316
参考文献
Abramovitch; Shapiro
Journal of the Chemical Society, 1956 , p. 4589,4591
反应条件
potassium hydroxide in ethanol
6 h; Heating;
参考文献
Guengoer, Timur; Malabre, Patrice; Teulon, Jean-Marie; Camborde, Francoise; Meignen, Joelle; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 25 p. 4307 - 4316
