1: 2,4-dichlorotriisopropylsilyloxybenzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
2: N,N-dimethyl-formamide in tetrahydrofuran; hexane
T=-68 - -10°C;
3: With hydrogenchloride; sodium chloride
Title compound not separated from byproducts;
参考文献
Von Hirschheydt, Thomas; Voss, Edgar
Synthesis, 2004 , # 12 p. 2062 - 2065