1-[(磷酰氧基)甲基]乙烷-1,2-二基二硬脂酸酯合成路线 (共 9 条)
参考文献
Olley
Chemistry and Industry (London, United Kingdom), 1954 , p. 1069
参考文献
Olley
Chemistry and Industry (London, United Kingdom), 1954 , p. 1069
参考文献
Olley
Chemistry and Industry (London, United Kingdom), 1954 , p. 1069
参考文献
Chemistry and Industry (London, United Kingdom), , p. 1069
反应条件
water in methanol
T=50°C; 2 h;
参考文献
Nifantyev, E. E.; Predvoditelev, D. A.; Fursenko, I. V.; Smirnova, L. I.
Synthesis, 1982 , # 2 p. 132 - 134
反应条件
1: 1.5 h / 120 °C / atmosphere of dry argon
2: 1.5 h / 120 °C / atmosphere of dry argon
3: iodosylbenzene / benzene / 1 h / 18 - 20 °C
4: NaI / acetone / 1.5 h / Heating
5: KRS-40T resin in H+ form / CHCl3; methanol; H2O / 0.25 h / 18 - 20 °C
6: 42 percent / H2 / palladium black / CHCl3; methanol / 1 h
View Scheme
参考文献
Smirnova, L.I.; Malenkovskaya, M. A.; Predvoditelev, D. A.; Nifant'ev, E. E.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1011 - 1019
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1170 - 1179
反应条件
1: NaI / acetonitrile / 3 h / 60 °C
2: 56 percent / water / methanol / 2 h / 50 °C
View Scheme
参考文献
Nifantyev, E. E.; Predvoditelev, D. A.; Fursenko, I. V.; Smirnova, L. I.
Synthesis, 1982 , # 2 p. 132 - 134
反应条件
hydrogen; platinum(IV) oxide
参考文献
Bevan at al.,T.H.
Journal of the Chemical Society, 1962 , p. 3495 - 3498
参考文献
Kabashima
Chemische Berichte, 1938 , vol. 71, p. 1072