7beta-羟基胆固醇3beta-乙酸酯合成路线 （共 14 条）
反应条件
sodium tetrahydroborate; cerium (III) chloride heptahydrate in tetrahydrofuran; methanol T=20°C; 0.25 h;
参考文献
Carvalho, Joao F. S.; Silva, M. Manuel Cruz; Moreira, Joao N.; Simoes, Sergio; Sa E Melo, M. Luisa
Journal of Medicinal Chemistry, 2010 , vol. 53, # 21 p. 7632 - 7638
反应条件
ferric picolinate complexes; dihydrogen peroxide in acetonitrile 3 h; Ambient temperature; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 4 p. 750 - 752
反应条件
sodium tetrahydroborate in 1,4-dioxane 5 h; other time (22 h), various solvents (n-PrOH, C6H6-EtOH); stereospecific reduction of 7-oxo group in 3β-acetoxycholest-5-en-7-one; Product distribution;
参考文献
Synthetic Communications, , vol. 19, # 3and4 p. 439 - 442
反应条件
T=160°C; 1 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2325 - 2328
反应条件
potassium carbonate in diethyl ether
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 916 - 923
参考文献
Journal of the Chemical Society, , p. 1798,1800
反应条件
T=160°C; 1 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2325 - 2328
反应条件
ferric picolinate complexes; dihydrogen peroxide in acetonitrile 3 h; Ambient temperatureother 3β-acetoxy-Δ5-steroids; Mechanism;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 4 p. 750 - 752
反应条件
7,8,10-trimethylisoalloxazine; oxygen in acetonitrile 12 h; Irradiation; Product distribution; Further Variations:Reagentsreaction times;
参考文献
Shuping, Wu; Zhiqin, Jiang; Heting, Li; Li, Yang; Daixun, Zeng
Molecules, 2001 , vol. 6, # 1 p. 52 - 60
参考文献
Journal of the Chemical Society, , p. 1798,1800
