反应条件
1: SOCl2 / benzene / 1 h / Heating
2: diethyl ether / Ambient temperature
3: 74 percent / LAH / dioxane; diethyl ether
4: 1.) SOCl2 / 1.) benzene, reflux, 2.) ether, r.t.
5: 1.) POCl3, 2.) KI / 1.) reflux, 2 h, 2.) H2O
6: NaBH4 / methanol / 1 h
View Scheme
参考文献
Nagarajan, K.; Talwalker, P. K.; Kulkarni, C. L.; Shah, R. K.; Shenoy, S. J.; Prabhu, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 83 - 97
