6-(Z-氨基)-1-己醇合成路线 （共 17 条）
反应条件
1: 70 percent / pyridine 2: 92 percent / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 9 p. 713 - 716
反应条件
1: thionyl chloride 2: lithium aluminium tetrahydride View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 4 p. 1018 - 1029
反应条件
1.) CH2Cl2, 1 h, room temp. 2.) CH2Cl2; Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 7 p. 555 - 556
反应条件
lithium borohydride; chloro-trimethyl-silane in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Giannis, Athanassios; Sandhoff, Konrad
Angewandte Chemie, 1989 , vol. 101, # 2 p. 220 - 222
反应条件
4-(polystyrylMeO)-2,2,6,6-tetraMepiperidin-1-yloxy radical; PS-CH2Me3(+)*ClO2(-); PS-CH2NMe3(+)*H2PO4(-); potassium bromide in water; acetonitrile T=20°C; 36 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 8 p. 1024 - 1025
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Journal of the American Chemical Society, , vol. 126, # 14 p. 4543 - 4549
反应条件
1: 63.5 percent
2: 94.6 percent / NaI
View Scheme
参考文献
Chipowsky,S.; Lee,Y.C.
Carbohydrate Research, 1973 , vol. 31, p. 339 - 346
