4-(Z-氨基)-1-丁醇合成路线 （共 16 条）
反应条件
sodium carbonate in tetrahydrofuran; water T=0 - 20°C;
参考文献
Kometani, Miki; Ihara, Kohki; Kimura, Rumi; Kinoshita, Hideki
Bulletin of the Chemical Society of Japan, 2009 , vol. 82, # 3 p. 364 - 380
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen in tert-butyl alcohol T=80°C; P=22502.3 Torr; 24 h; Autoclave;
参考文献
Ito, Masato; Koo, Lee Wei; Himizu, Akio; Kobayashi, Chika; Sakaguchi, Ayaka; Ikariya, Takao
Angewandte Chemie - International Edition, 2009 , vol. 48, # 7 p. 1324 - 1327
反应条件
triethylamine in acetone T=20°C; 7 h;
参考文献
Wakamiya, Tateaki; Kinoshita, Tomohiko; Hattori, Yoshihide; Yamaguchi, Yoshihiro; Naoki, Hideo; Corzo, Gerardo; Nakajimal, Terumi
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 2 p. 331 - 340
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Liu, Jian-Dong; Chen, Ying-Chun; Zhang, Guo-Biao; Li, Zhi-Qiang; Chen, Peng; Du, Ji-Yuan; Tu, Yong-Qiang; Fan, Chun-An
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2721 - 2730
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran T=65°C; 0.25 h; 2: With methanol in tetrahydrofuran T=65°C;
参考文献
Goncalves; Pinheiro; Da Silva; Da Costa; Kaiser; De Souza
Synthetic Communications, 2011 , vol. 41, # 9 p. 1276 - 1281
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Fernandez; Menendez; Gotor
Synthesis, 1991 , # 9 p. 713 - 716
反应条件
1: 70 percent / pyridine 2: 90 percent / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 9 p. 713 - 716
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Boseggia, Elisa; Gatos, Maddalena; Lucatello, Lorena; Mancin, Fabrizio; Moro, Stefano; Palumbo, Manlio; Sissi, Claudia; Tecilla, Paolo; Tonellato, Umberto; Zagotto, Giuseppe
Journal of the American Chemical Society, 2004 , vol. 126, # 14 p. 4543 - 4549
反应条件
triphenylphosphine in dichloromethane
参考文献
Meiji Seika Kaisha Ltd.
Patent: US6576627 B1, 2003 ;
反应条件
triphenylphosphine in tetrahydrofuran; hexane; ethyl acetate
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4604402 A1, 1986 ;
US 4604402 A
Title/Abstract Full Text Show Details
E. R. Squibb and Sons, Inc.
Patent: US4621092 A1, 1986 ;
US 4621092 A
