2-三正丁基甲锡烷基吡啶合成路线 (共 97 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 48 h; Heating;
参考文献
Zoltewicz, John A.; Maier, Nobert M.; Fabian, Walter M.F.
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3215 - 3219
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 16 h; Heating;
参考文献
Fallahpour, Reza-Ali; Neuburger, Markus
European Journal of Organic Chemistry, 2001 , # 10 p. 1853 - 1856
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine in toluene 72 h; RefluxInert atmosphereSchlenk technique;
参考文献
Otte, Matthias; Kuijpers, Petrus F.; Troeppner, Oliver; Ivanovic-Burmazovic, Ivana; Reek, Joost N. H.; De Bruin, Bas
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10170 - 10178
反应条件
triphenyl-arsane; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane T=50°C; Stille cross-coupling;
参考文献
El Akkaoui; Koubachi; El Kazzouli; Berteina-Raboin; Mouaddib; Guillaumet
Tetrahedron Letters, 2008 , vol. 49, # 15 p. 2472 - 2475
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 16 h; Heating;
参考文献
Fallahpour, Reza-Ali; Neuburger, Markus
European Journal of Organic Chemistry, 2001 , # 10 p. 1853 - 1856
反应条件
1: 340 mg / Pd(Ph3P)4 / toluene / 72 h / Heating 2: 64 percent / K2CO3 / Pd(Ph3P)4 / tetrahydrofuran; H2O / 14 h / Heating View Scheme
参考文献
Zoltewicz, John A.; Maier, Nobert M.; Fabian, Walter M.F.
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3215 - 3219
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 24 h; Heating;
参考文献
Zoltewicz, John A.; Maier, Nobert M.; Fabian, Walter M.F.
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3215 - 3219
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; 16 h;
参考文献
Fallahpour, Reza-Ali
European Journal of Inorganic Chemistry, 1998 , # 9 p. 1205 - 1207
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=110°C; Stille cross-coupling; 18 h; Inert atmosphere;
参考文献
Verniest, Guido; Wang, Xingpo; De Kimpe, Norbert; Padwa, Albert
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 424 - 433
反应条件
palladium diacetate; copper dichloride in tetrahydrofuran T=23°C; 1 h;
参考文献
Parrish, Jay P.; Flanders, Vincent L.; Floyd, Ryan J.; Jung, Kyung Woon
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7729 - 7731