2-三正丁基甲锡烷基吡啶合成路线 （共 97 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide 1) DMF, 5 min, 100 deg C, 2) DMF, 120-140 min, 100 deg C; Yield given. Multistep reaction;
参考文献
Malm, Johan; Bjoerk, Patrick; Gronowitz, Salo; Hoernfeldt, Anna-Britta
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2199 - 2202
反应条件
(Ph3Ph)4Pd in toluene T=110°C; Substitution; Stille coupling; 16 h;
参考文献
Synthesis, , # 8 p. 1138 - 1142
反应条件
dinitrogen tetraoxide in tetrachloromethane; dimethyl sulfoxide T=20°C; 16 h;
参考文献
Fargeas, Valerie; Favresse, Fabien; Mathieu, Didier; Beaudet, Isabelle; Charrue, Pierre; Lebret, Bruno; Piteau, Marc; Quintard, Jean-Paul
European Journal of Organic Chemistry, 2003 , # 9 p. 1711 - 1721
反应条件
dinitrogen tetraoxide in tetrachloromethane; dimethyl sulfoxide T=20°C; Nitration; substitution; 16 h; dark;
参考文献
Favresse, Fabien; Fargeas, Valerie; Charrue, Pierre; Lebret, Bruno; Piteau, Marc; Quintard, Jean-Paul
Journal of Organometallic Chemistry, 2000 , vol. 598, # 1 p. 187 - 190
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=120°C;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2005/5435 A1, 2005 ;
Location in patent: Page/Page column 36 ;
WO 2005/005435 A1
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille reaction; 24 h; Heating;
参考文献
Berghian, Camelia; Darabantu, Mircea; Turck, Alain; Ple, Nelly
Tetrahedron, 2005 , vol. 61, # 40 p. 9637 - 9644
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=110°C; Substitution; Stille reaction; 16 h;
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=110°C; Stille cross-coupling; 18 h; Inert atmosphere;
参考文献
Verniest, Guido; Wang, Xingpo; De Kimpe, Norbert; Padwa, Albert
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 424 - 433
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=105°C; Stille cross-coupling; 6 h;
参考文献
Verniest, Guido; Wang, Xingpo; De Kimpe, Norbert; Padwa, Albert
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 424 - 433
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille coupling; 40 h; Heating;
参考文献
Zong, Ruifa; Thummel, Randolph P.
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 10800 - 10801
