1,3-二(3-羟基丙基)-1,1,3,3-四甲基二硅氧烷合成路线 （共 16 条）
反应条件
potassium carbonate in methanol T=20°C; 2 h;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 85-86, p. 149 - 155
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene T=20°C; 4 h; Reflux;
参考文献
Frampton, Mark B.; Subczynska, Izabela; Zelisko, Paul M.
Biomacromolecules, 2010 , vol. 11, # 7 p. 1818 - 1825
18547-30-32,2,7,7,9,9,14,14-八甲基-3,8,13-三氧杂-2,7,9,14-四硅杂十五烷
→
反应条件
hydrogenchloride in diethyl ether T=25°C; 15 h;
参考文献
Journal of Organometallic Chemistry, , vol. 332, p. 63 - 68
反应条件
formate dehydrogenase; water 17 h; Enzymatic reaction;
参考文献
Froehlich, Peter; Albert, Kristin; Bertau, Martin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7941 - 7950
反应条件
hydrogenchloride; acetone
参考文献
Journal of the American Chemical Society, , vol. 80, p. 4106
18547-30-32,2,7,7,9,9,14,14-八甲基-3,8,13-三氧杂-2,7,9,14-四硅杂十五烷
→
反应条件
water; toluene-4-sulfonic acid 2 h; Heating;
参考文献
Pusztai, Erika; Nagy, Jozsef; Wagner, Oedoen
Main Group Metal Chemistry, 2012 , vol. 35, # 3-4 p. 91 - 97
反应条件
1: sodium 2: aqueous HCl; acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 80, p. 4106
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 35, p. 4180 - 4183
反应条件
1: aq. H2SO4 2: LiAlH4 / diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 35, p. 4180 - 4183
反应条件
dihydrogen hexachloroplatinate in isopropyl alcohol; toluene T=100°C; 6 h; Title compound not separated from byproducts;
参考文献
Revue Roumaine de Chimie, , vol. 46, # 7 p. 703 - 711
