4-甲氧基-2(1H)-嘧啶酮合成路线 （共 10 条）
反应条件
triethylamine in toluene T=20°C; 24 h;
参考文献
Corsaro, Antonino; Pistara, Venerando; Rescifina, Antonio; Chiacchio, Maria A.; Piperno, Anna; Romeo, Giovanni
Heterocycles, 2005 , vol. 65, # 5 p. 1079 - 1097
反应条件
ethanol; water; dihydrogen peroxide
参考文献
Chi; Chen
Huaxue Xuebao, 1956 , vol. 22, p. 194,199
Scientia Sinica (English Edition), 1957 , vol. 6, p. 111,118
Chem.Abstr., 1957 , p. 16485
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide T=60°C; 0.5 h; 2: dimethyl sulfate in N,N-dimethyl-formamide T=60°C; 48 h;
参考文献
Tetrahedron, , vol. 62, # 29 p. 6848 - 6854
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide T=60°C; 0.5 h; 2: diethyl sulphate in N,N-dimethyl-formamide T=60°C; 48 h;
参考文献
Gambacorta, Augusto; Tofani, Daniela; Loreto, Maria Antonietta; Gasperi, Tecla; Bernini, Roberta
Tetrahedron, 2006 , vol. 62, # 29 p. 6848 - 6854
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide T=60°C; 0.5 h; 2: dimethyl sulfate in N,N-dimethyl-formamide T=60°C; 48 h;
参考文献
Tetrahedron, , vol. 62, # 29 p. 6848 - 6854
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide T=60°C; 0.5 h; 2: dimethyl sulfate in N,N-dimethyl-formamide T=60°C; 48 h;
参考文献
Tetrahedron, , vol. 62, # 29 p. 6848 - 6854
反应条件
Yield given. Multistep reaction;
参考文献
Alexander, Petr; Holy, Antonin
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, p. 1151 - 1163
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide
T=60°C; 0.5 h;
2: diethyl sulphate in N,N-dimethyl-formamide
T=60°C; 48 h;
参考文献
Gambacorta, Augusto; Tofani, Daniela; Loreto, Maria Antonietta; Gasperi, Tecla; Bernini, Roberta
Tetrahedron, 2006 , vol. 62, # 29 p. 6848 - 6854
反应条件
1: 4-Methoxy pyrimidin-2-one With lithium hydride in N,N-dimethyl-formamide
T=60°C; 0.5 h;
2: dimethyl sulfate in N,N-dimethyl-formamide
T=60°C; 48 h;
参考文献
Gambacorta, Augusto; Tofani, Daniela; Loreto, Maria Antonietta; Gasperi, Tecla; Bernini, Roberta
Tetrahedron, 2006 , vol. 62, # 29 p. 6848 - 6854
反应条件
in 1,4-dioxane
Heating;
参考文献
Chalupova, Sarka; Holy, Antonin; Masojidkova, Milena
Collection of Czechoslovak Chemical Communications, 2005 , vol. 70, # 12 p. 2053 - 2065
