9,10-二氢-9-蒽基(三甲基)硅烷合成路线 （共 14 条）
反应条件
n-butyllithium 1) THF, -78 deg C; Yield given. Multistep reaction;
参考文献
Studer, Armido; Amrein, Stephan; Schleth, Florian; Schulte, Tobias; Walton, John C.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5726 - 5733
反应条件
ammonia; lithium in tetrahydrofuran T=-78°C; 0.5 h; Yield given;
参考文献
Marcinow, Z.; Clawson, D. K.; Rabideau, P. W.
Tetrahedron, 1989 , vol. 45, # 17 p. 5441 - 5448
参考文献
Maienthal et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 6392
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Petrow; Tschernyschewa
Doklady Akademii Nauk SSSR, 1952 , vol. 84, p. 515,516
Chem.Abstr., 1953 , p. 3288
反应条件
Li in not given (CH3)3SiH, anthracene and Li; hydrolysis;;
参考文献
Petrov, A. D.; Cernyseva, T. I.
Doklady Akademii Nauk SSSR, 1952 , vol. 84, p. 515 - 518
C. A., 1953 , p. 3288
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Gmelin Handbook: Si: MVol.C, 29, page 90 - 93
反应条件
lithium 1) diethyl ether, benzene, r.t., 90 h, 2) 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Daney, Michele; Lapouyade, Rene; Bouas-Laurent, Henri
Journal of Organic Chemistry, 1983 , vol. 48, p. 5055 - 5062
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-30°C; 2 h;
参考文献
Marcinow, Z.; Clawson, D. K.; Rabideau, P. W.
Tetrahedron, 1989 , vol. 45, # 17 p. 5441 - 5448
反应条件
n-butyllithium
1) THF, 0 deg C, 1.3 h, 2) 0 deg C, 30 min, then RT, 90 min; Yield given. Multistep reaction;
参考文献
Dhar, Raj K.; Clawson, D. K.; Fronczek, Frank R.; Rabideau, Peter W.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2917 - 2921
反应条件
n-butyllithium
1) THF, 0 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Rabideau, Peter W.; Dhar; Clawson; Zhan, Zhengyun
Tetrahedron Letters, 1991 , vol. 32, # 32 p. 3969 - 3972
反应条件
n-butyllithium
1) THF, 0 deg C, 1.3 h, 2) 0 deg C, 30 min, then RT, 90 min; Yield given. Multistep reaction;
参考文献
Dhar, Raj K.; Clawson, D. K.; Fronczek, Frank R.; Rabideau, Peter W.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2917 - 2921
反应条件
n-butyllithium
1) THF, 0 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Rabideau, Peter W.; Dhar; Clawson; Zhan, Zhengyun
Tetrahedron Letters, 1991 , vol. 32, # 32 p. 3969 - 3972
