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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-萘-2-基哌啶
合成路线
（共 5 条）
1421065-81-7
→
反应条件
180160-99-0
4-萘-2-基哌啶
反应条件
hydrogenchloride in ethyl acetate T=25°C; 5 h;
参考文献
ABBOTT LABORATORIES; ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.; WANG, Xueqing; MEYER, Michael; YAO, Betty; GUO, Tao; WEI, Guo Ping,Robert; WANG, Lijuan, Jane
Patent: WO2013/10453 A1, 2013 ;
Location in patent: Page/Page column 173 ;
580-13-2
2-溴代萘
→
反应条件
180160-99-0
4-萘-2-基哌啶
反应条件
暂无反应条件数据
参考文献
Eli Lilly and Company
Patent: US6303627 B1, 2001 ;
US 6303627 B1
79099-07-3
N-叔丁氧羰基-4-哌啶酮
→
反应条件
180160-99-0
4-萘-2-基哌啶
反应条件
1: lithium hexamethyldisilazane / tetrahydrofuran / 6 h / -78 - 20 °C / |Inert atmosphere 2: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / ethylene glycol dimethyl ether / 16 h / |Reflux 3: palladium on activated charcoal; hydrogen / methanol / 24 h / 2585.81 Torr 4: hydrogenchloride / ethyl acetate / 5 h / 25 °C View Scheme
参考文献
ABBOTT LABORATORIES; ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.; WANG, Xueqing; MEYER, Michael; YAO, Betty; GUO, Tao; WEI, Guo Ping,Robert; WANG, Lijuan, Jane
Patent: WO2013/10453 A1, 2013 ;
138647-49-1
3,6-二氢-4-[[(三氟甲基)磺酰]氧基]-1(2H)-吡啶甲酸叔丁酯
→
反应条件
180160-99-0
4-萘-2-基哌啶
反应条件
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / ethylene glycol dimethyl ether / 16 h / |Reflux 2: palladium on activated charcoal; hydrogen / methanol / 24 h / 2585.81 Torr 3: hydrogenchloride / ethyl acetate / 5 h / 25 °C View Scheme
参考文献
ABBOTT LABORATORIES; ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.; WANG, Xueqing; MEYER, Michael; YAO, Betty; GUO, Tao; WEI, Guo Ping,Robert; WANG, Lijuan, Jane
Patent: WO2013/10453 A1, 2013 ;
194669-56-2
→
反应条件
180160-99-0
4-萘-2-基哌啶
反应条件
1: palladium on activated charcoal; hydrogen / methanol / 24 h / 2585.81 Torr 2: hydrogenchloride / ethyl acetate / 5 h / 25 °C View Scheme
参考文献
ABBOTT LABORATORIES; ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.; WANG, Xueqing; MEYER, Michael; YAO, Betty; GUO, Tao; WEI, Guo Ping,Robert; WANG, Lijuan, Jane
Patent: WO2013/10453 A1, 2013 ;
