1,4-二甲基-9H-咔唑合成路线 （共 61 条）
反应条件
in ethanol
96 h; Irradiation;
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 47 percent / 5 h / 150 °C
2: 87 percent / Pd/C 5 percent / various solvent(s) / 3 h / Heating
View Scheme
参考文献
Mustafin; Khalilov; Ismagilov; Baimetov; Spirikhin; Abdrakhmanov; Tolstikov
Russian Chemical Bulletin, 1999 , vol. 48, # 11 p. 2121 - 2126
反应条件
1: 88 percent
2: 59 percent / K2CO3, copper bronze / 7 h / 180 °C
3: 97 percent / KOH / ethanol / 2 h / Heating
4: 53 percent / ethanol / 96 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 74 percent / K2CO3, copper bronze / 7 h / 180 °C
2: 65 percent / KOH / ethanol / 2 h
3: 47 percent / ethanol / 48 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 59 percent / K2CO3, copper bronze / 7 h / 180 °C
2: 97 percent / KOH / ethanol / 2 h / Heating
3: 53 percent / ethanol / 96 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 65 percent / KOH / ethanol / 2 h
2: 47 percent / ethanol / 48 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 97 percent / KOH / ethanol / 2 h / Heating
2: 53 percent / ethanol / 96 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Hughes, David; Hursthouse, Michael B.; Lewis, Rhiannon
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 669 - 673
反应条件
1: 91 percent
2: 87 percent / K2CO3, copper bronze / 7 h / 160 °C
3: 90 percent / KOH / ethanol / 2 h / Heating
4: ethanol / 84 h / Irradiation
View Scheme
参考文献
Groundwater, Paul W.; Lewis, Rhiannon
Journal of Chemical Research, Miniprint, 1995 , # 6 p. 1477 - 1486
反应条件
Amberlyst 15 in isopropyl alcohol
1.5 h; Reflux;
参考文献
Ballini, Roberto; Gabrielli, Serena; Palmieri, Alessandro; Petrini, Marino
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2459 - 2462
反应条件
pyridine hydrochloride; (carboxymethyl)trimethylammonium chloride hydrazide
1.) reflux, 1 h, 2.) ethanol/acide acetique, reflux; Yield given. Multistep reaction;
参考文献
Bisagni, Emile; Ducrocq, Claire; Hung, Nguyen Chi
Tetrahedron, 1980 , vol. 36, p. 1327 - 1330
