6 - 甲氧基-1,4 - 二甲基-9H-咔唑合成路线 （共 15 条）
反应条件
montmorillonite K-10 T=90°C; 0.05 h; microwave heating;
参考文献
Abid, Mohammed; Spaeth, Andrew; Toeroek, Bela
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 15 p. 2191 - 2196
反应条件
montmorillonite K-10 T=160°C; Friedel Crafts alkylation; 1 h; Microwave irradiationneat (no solvent);
参考文献
Kulkarni, Aditya; Quang, Phong; Toeroek, Bela
Synthesis, 2009 , # 23 art. no. M02409SS, p. 4010 - 4014
反应条件
1: 45 percent / copper bronze, K2CO3 / 4 h / Heating 2: 73 percent / ethanol / 7 h / Irradiation View Scheme
参考文献
Hall, Robin J.; Marchant, Jeremy; Oliveira-Campos, Ana M. F.; Queiroz, Maria-Joao R. P.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3439 - 3450
反应条件
1: 45 percent / copper bronze, K2CO3 / 4 h / Heating 2: 73 percent / ethanol / 7 h / Irradiation View Scheme
参考文献
Hall, Robin J.; Marchant, Jeremy; Oliveira-Campos, Ana M. F.; Queiroz, Maria-Joao R. P.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3439 - 3450
反应条件
toluene-4-sulfonic acid
参考文献
Caruso, Anna; Chimento, Adele; El-Kashef, Hussein; Lancelot, Jean-Charles; Panno, Antonella; Pezzi, Vincenzo; Saturnino, Carmela; Sinicropi, Maria Stefania; Sirianni, Rosa; Rault, Sylvain
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 4 p. 609 - 613
反应条件
1: 60 percent / phosphorus oxychloride / trichloroethene / 4 h / 100 °C 2: 87 percent View Scheme
参考文献
Martin-Onraet; Gansser; Plat; et al.
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 10 p. 745 - 754
反应条件
1: N-methyl-N-formyl-aniline With trichlorophosphate in 1,2-dichloro-benzene T=20°C; Vilsmeier-Haack reaction; 1.5 h; 2: 1,4-dimethyl 6-methoxy 9H-carbazole in 1,2-dichloro-benzene T=105°C; Vilsmeier-Haack reaction; 4 h; 3: With water; sodium acetate in 1,2-dichloro-benzene T=20°C;
参考文献
Vehar, Blaz; Hrast, Martina; Kovac, Andreja; Konc, Janez; Mariner, Katherine; Chopra, Ian; O'Neill, Alex; Janezic, Dusanka; Gobec, Stanislav
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5137 - 5146
反应条件
trichlorophosphate in 1,1,2-trichloroethylene T=100°C; 4 h;
参考文献
Martin-Onraet; Gansser; Plat; et al.
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 10 p. 745 - 754
反应条件
trichlorophosphate in chlorobenzene 6.5 h; Reflux;
参考文献
Deane, Fiona M.; Miller, Charlotte M.; Maguire, Anita R.; McCarthy, Florence O.
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 4 p. 814 - 823
反应条件
sodium iodide in acetonitrile 1 h; Heating;
参考文献
Harada, Naoyuki; Ozaki, Kunihiko; Oda, Kouji; Nakanishi, Noriyuki; Ohashi, Motoaki; Hashiyama, Tomiki; Tsujihara, Kenji
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1156 - 1162
