甲基2,3,6-三-O-乙酰基吡喃己糖苷合成路线 (共 23 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol P=760 Torr; 3 h;
参考文献
Carbohydrate Research, , vol. 102, p. 147 - 158
反应条件
acetic acid in toluene T=80°C; 16 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 6 p. 1069 - 1080
反应条件
hydrogen; Lindlar's catalyst in methanol T=20°C; 3 h;
参考文献
Carbohydrate Research, , vol. 337, # 2 p. 87 - 91
反应条件
1: methyl-α-D-glucopyranoside With di(n-butyl)tin oxide in methanol 2 h; Heating; 2: acetic anhydride in acetonitrile T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 72, # 4 p. 1499 - 1502
反应条件
1: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water T=20°C; 6 h; 2: With ytterbium(III) triflate in dichloromethane T=20°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2299 - 2301
反应条件
VO(OTf)2 in methanol; dichloromethane T=55°C; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 1 p. 299 - 302
反应条件
1: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water T=20°C; 6 h; 2: With ytterbium(III) triflate in dichloromethane T=20°C; 3 h; Further stages.;
参考文献
Tetrahedron, , vol. 63, # 45 p. 10921 - 10929
反应条件
rabbit serum (esterase) in various solvent(s) T=37°C; 3 h;
参考文献
Tetrahedron, , vol. 49, # 47 p. 10977 - 10986
反应条件
4 A molecular sieve T=0°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 44, # 25 p. 4661 - 4663