1H-茚-1-基三甲基硅烷合成路线 （共 14 条）
反应条件
1: CH2-indene With n-butyllithium 2: chloro-trimethyl-silane Further stages.;
参考文献
Moeller, Andreas C.; Heyn, Richard H.; Blom, Richard; Swang, Ole; Goerbitz, Carl Henrik; Kopf, Juergen
Dalton Transactions, 2004 , # 10 p. 1578 - 1589
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138
反应条件
NaOH in sodium hydroxide byproducts: indene; aq. NaOH; C9H6(Si(CH3)3)2 in 20percent aq. NaOH at 100°C;;
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138
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Gmelin Handbook: Si: MVol.C, 32, page 100 - 103
反应条件
1: CH2-indene With n-butyllithium in diethyl ether T=0°C; 2: SiMe3-halide in diethyl ether T=0°C;
参考文献
Grimmer, Neil E.; Coville, Neil J.; De Koning, Charles B.; Smith, Jeremy M.; Cook, Leanne M.
Journal of Organometallic Chemistry, 2000 , vol. 616, # 1-2 p. 112 - 127
反应条件
(CH3)3SiCl in tetrahydrofuran addn.;
参考文献
Merola, Joseph S.; Kacmarcik, Raymond T.
Organometallics, 1989 , vol. 8, p. 778 - 784
参考文献
Sommer; Marans
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135,5136
反应条件
tetrakis(triphenylphosphine) palladium(0)
参考文献
Trost, Barry M.; Keinan, Ehud
Tetrahedron Letters, 1980 , vol. 21, p. 2595 - 2598
反应条件
Br2 in not given at 20°C;;
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138
反应条件
1: 86 percent / dioxane dibromide / tetrahydrofuran / -78 deg C to room temperature 2: 67 percent / m-chloroperbenzoic acid / CH2Cl2 / 24 h / 5 °C 3: 52 percent / Bh3SnH, azoisobutyronitrile / tetrahydrofuran / 10 h / Heating View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
