2-乙酰基-3,5-双(苄氧基)苯酚合成路线 (共 35 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; Condensation; 1 h;
参考文献
Huang, Chusheng; Zhang, Zhe; Li, Shuhua; Li, Yulin
Journal of Chemical Research - Part S, 1999 , # 2 p. 148 - 149
反应条件
titanium tetrachloride in dichloromethane T=-5°C; 1.5 h;
参考文献
Bazin, Marc-Antoine; Bodero, Lizeth; Tomasoni, Christophe; Rousseau, Benedicte; Roussakis, Christos; Marchand, Pascal
European Journal of Medicinal Chemistry, 2013 , vol. 69, p. 823 - 832
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Kim, Mi Kyoung; Yoon, Hyunjun; Barnard, Dale Lynn; Chong, Youhoon
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 4 p. 486 - 488
反应条件
potassium carbonate in N,N,N',N',N'',N''-hexamethylphosphoric triamide; water
参考文献
Zaveri, Nurulain; Chao, Wan-Ru; Bensari, Ahlem
Patent: US2004/192723 A1, 2004 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=0 - 25°C;
参考文献
Kumazawa; Kimura; Matsuba; Sato; Onodera
Carbohydrate Research, 2001 , vol. 334, # 3 p. 183 - 193
反应条件
pyridine; potassium hydroxide in diethylene glycol T=120°C; 4 h;
参考文献
Caldwell, Stuart T.; Petersson, Hanna M.; Farrugia, Louis J.; Mullen, William; Crozier, Alan; Hartley, Richard C.
Tetrahedron, 2006 , vol. 62, # 31 p. 7257 - 7265
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=20 - 80°C; 1 - 7 h; 2: With hydrogenchloride; water in N,N-dimethyl-formamide Product distribution / selectivity;
参考文献
WO2007/2877 A1, ;
Page/Page column 7; 21-23 ;
反应条件
in N,N-dimethyl-formamide
反应条件
potassium carbonate in N,N-dimethyl-formamide T=150 - 153°C; 0.666667 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, p. 136 - 141
反应条件
potassium carbonate in N,N-dimethyl-formamide 6 h; Reflux;
参考文献
Sagrera, Gabriel; Seoane, Gustavo
Synthesis, 2010 , # 16 art. no. M06509SS, p. 2776 - 2786