2-苯基呋喃并[3,2-b]吡啶合成路线 （共 10 条）
反应条件
hydrogenchloride in acetone T=60°C; 4 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Di Giuseppe, Sabrina; Fabrizi, Giancarlo; Marinelli, Fabio
Organic Letters, 2002 , vol. 4, # 14 p. 2409 - 2412
反应条件
tetrabutyl-ammonium chloride; sodium acetate; palladium diacetate in N,N-dimethyl-formamide T=140°C; Sonogashira coupling; 0.25 h; microwave irradiation;
参考文献
Sorensen, Ulrik S.; Pombo-Villar, Esteban
Tetrahedron, 2005 , vol. 61, # 10 p. 2697 - 2703
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)pyridine-2,6-diamine; caesium carbonate in N,N-dimethyl-formamide T=130°C; Sonogashira Cross-Coupling; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Zhou, Rong; Wang, Wei; Jiang, Zhi-Jie; Wang, Kun; Zheng, Xue-Li; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
Chemical Communications, 2014 , vol. 50, # 45 p. 6023 - 6026
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)pyridine-2,6-diamine; caesium carbonate in N,N-dimethyl-formamide T=130°C; Sonogashira Cross-Coupling; 8 h; Schlenk techniqueInert atmosphere;
参考文献
Zhou, Rong; Wang, Wei; Jiang, Zhi-Jie; Wang, Kun; Zheng, Xue-Li; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
Chemical Communications, 2014 , vol. 50, # 45 p. 6023 - 6026
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=120°C; 24 h;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Watanabe, Ryo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2719 - 2724
反应条件
hydrogen bromide Heating;
参考文献
Beugelmans, Rene; Bois-Choussy, Michele
Heterocycles, 1987 , vol. 26, # 7 p. 1863 - 1871
反应条件
1: 80 percent / PdCl2(PPh3)2; CuI; Et3N / tetrahydrofuran / 5 h / 20 °C 2: 45 percent / NaHCO3 / methanol / 4 h / 20 °C View Scheme
参考文献
Arcadi, Antonio; Cacchi, Sandro; Di Giuseppe, Sabrina; Fabrizi, Giancarlo; Marinelli, Fabio
Organic Letters, 2002 , vol. 4, # 14 p. 2409 - 2412
反应条件
1: 80 percent / PdCl2(PPh3)2; CuI; Et3N / tetrahydrofuran / 5 h / 20 °C 2: 45 percent / NaHCO3 / methanol / 4 h / 20 °C View Scheme
参考文献
Arcadi, Antonio; Cacchi, Sandro; Di Giuseppe, Sabrina; Fabrizi, Giancarlo; Marinelli, Fabio
Organic Letters, 2002 , vol. 4, # 14 p. 2409 - 2412
反应条件
1: K2CO3 / dimethylformamide / 2 h / 80 °C 2: 70 percent / t-C4H9OK / liquid ammonia / 6 h / Irradiation 3: 100 percent / 45percent aq.HBr / Heating View Scheme
参考文献
Beugelmans, Rene; Bois-Choussy, Michele
Heterocycles, 1987 , vol. 26, # 7 p. 1863 - 1871
参考文献
Mladenovic,S.A.; Castro,C.E.
Journal of Heterocyclic Chemistry, 1968 , vol. 5, p. 227 - 230
