2-甲氧基-4,6-二甲基苯胺合成路线 (共 9 条)
反应条件
ethanol; nickel
T=100°C; P=99293.6 Torr; Hydrogenation;
参考文献
Adams; Stewart
Journal of the American Chemical Society, 1941 , vol. 63, p. 2859,2861
反应条件
2-aminopyridine; copper(l) chloride in methanol; diethylene glycol dimethyl ether
T=85°C; Etherification; 24 h;
参考文献
Fagan, Paul J.; Hauptman, Elisabeth; Shapiro, Rafael; Casalnuovo, Albert
Journal of the American Chemical Society, 2000 , vol. 122, # 21 p. 5043 - 5051
反应条件
T=100°C; P=99293.6 Torr; Hydrogenation;
参考文献
Adams; Stewart
Journal of the American Chemical Society, 1941 , vol. 63, p. 2859,2861
反应条件
1: aqueous NaOH
2: sodium dithionite; aqueous ethanol / anschliessend Erhitzen des Reaktionsprodukts mit konz. wss. Salzsaeure
View Scheme
参考文献
Rowe et al.
Journal of the Society of Chemical Industry, London, 1930 , vol. 49, p. 469 T, 472 T
反应条件
1: glacial acetic acid; nitric acid / <5
2: aqueous NaOH
3: sodium dithionite; aqueous ethanol / anschliessend Erhitzen des Reaktionsprodukts mit konz. wss. Salzsaeure
View Scheme
参考文献
Rowe et al.
Journal of the Society of Chemical Industry, London, 1930 , vol. 49, p. 469 T, 472 T
参考文献
Rowe et al.
Journal of the Society of Chemical Industry, London, 1930 , vol. 49, p. 469 T, 472 T
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
反应条件
sulfuric acid; sodium sulfate
T=145°C; Diazotization;
参考文献
Cosgrove; Waters
Journal of the Chemical Society, 1949 , p. 3189,3193
参考文献
Teuber; Hasselbach
Chemische Berichte, 1959 , vol. 92, p. 674,688