3,3,3-三氟-2,2-二甲基丙酸合成路线 （共 4 条）
反应条件
sodium hydroxide; water; tetra(n-butyl)ammonium hydrogensulfate in dimethyl sulfoxide T=20°C; Hydrolysis; 48 h;
参考文献
Dmowski, Wojciech; Wolniewicz, Adam
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 141 - 146
反应条件
1: 61 percent / EtONa / ethanol 2: NaOH; H2O / 48 h / 20 °C 3: 56 percent / SF4 / 3 h / 30 °C 4: 88 percent / NaOH; H2O; Bu4NHSO4 / dimethylsulfoxide / 48 h / 20 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 102, # 1-2 p. 141 - 146
反应条件
1: NaOH; H2O / 48 h / 20 °C 2: 56 percent / SF4 / 3 h / 30 °C 3: 88 percent / NaOH; H2O; Bu4NHSO4 / dimethylsulfoxide / 48 h / 20 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 102, # 1-2 p. 141 - 146
反应条件
1: 56 percent / SF4 / 3 h / 30 °C 2: 88 percent / NaOH; H2O; Bu4NHSO4 / dimethylsulfoxide / 48 h / 20 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 102, # 1-2 p. 141 - 146
