4-甲氧基-2-硝基苯磺酰氯合成路线 (共 5 条)
反应条件
1: With hydrogenchloride; sodium nitrite T=0°C; 0.75 h; 2: With sulfur dioxide; acetic acid; copper dichloride 1.5 h;
参考文献
Journal of Medicinal Chemistry, , vol. 48, # 23 p. 7363 - 7373
反应条件
hydrogenchloride; nitric acid
参考文献
Gazzetta Chimica Italiana, , vol. 90, p. 1277 - 1289
反应条件
(i) aq. HCl, NaNO2, (ii) CuCl2, SO2, AcOH; Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 28, p. 1851 - 1856
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 28, # 9 p. 2005 - 2011
参考文献
Hayman,D.F. et al.
Journal of Pharmacy and Pharmacology, 1962 , vol. 14, p. 522 - 533
反应条件
triethylamine in dichloromethane; water
T=20°C; 36 h; Inert atmosphere;
参考文献
Miura, Tomoya; Yamauchi, Motoshi; Kosaka, Akira; Murakami, Masahiro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 29 p. 4955 - 4957