1,3,5-三(溴甲基)-2,4,6-三乙基苯合成路线 （共 8 条）
反应条件
hydrogen bromide; zinc dibromide in acetic acid Reflux;
参考文献
Aversa, Maria Chiara; Barattucci, Anna; Bonaccorsi, Paola
Synlett, 2011 , # 2 art. no. G31510ST, p. 254 - 258
反应条件
hydrogen bromide; zinc dibromide in acetic acid T=90 - 95°C; 60 h;
参考文献
Kim, Sung-Gon; Sambasivan, Sunderraman; Ann, Kyo Han
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 3 p. 724 - 726
反应条件
sulfuric acid; potassium bromide Yield given;
参考文献
Capitan-Vallvey, Luis Fermin; Arroyo-Guerrero, Eduardo; Fernandez-Ramos, Maria Dolores; Santoyo-Gonzalez
Analytical Chemistry, 2005 , vol. 77, # 14 p. 4459 - 4466
反应条件
1: HOAc; HBr 2: HOAc; KBr; H2SO4 View Scheme
参考文献
Voo; Lam; Rheingold; Riordan
Journal of the Chemical Society, Dalton Transactions, 2001 , # 12 p. 1803 - 1805
反应条件
1: 90 percent / AlCl3 / 12 h / 0 - 20 °C 2: 70 percent / HBr; Zn; AcOH / 48 h / 90 °C View Scheme
参考文献
Wallace, Karl J.; Hanes, Robert; Anslyn, Eric; Morey, Jeroni; Kilway, Kathleen V.; Siegel, Jay
Synthesis, 2005 , # 12 art. no. M09004SS, p. 2080 - 2083
反应条件
ammonium hydroxide in tetrahydrofuran; ethanol
参考文献
Ryu, Eui-Hyun; Yan, Jie; Zhong, Zhenqi; Zhao, Yan
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7205 - 7213
反应条件
N,N'-dimethyl-N,N'-propyleneurea; sodium azide
T=80°C; 12 h;
参考文献
Ryu, Eui-Hyun; Yan, Jie; Zhong, Zhenqi; Zhao, Yan
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7205 - 7213
反应条件
sodium azide in N,N-dimethyl-formamide
T=25°C; Substitution; 24 h;
参考文献
Niikura, Kenichi; Anslyn, Eric V.
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 12 p. 2769 - 2775
