(苯基氧代甲基)膦酸二甲酯合成路线 （共 52 条）
反应条件
(i) NaH, toluene, (ii) /BRN= 2050004/; Multistep reaction;
参考文献
Shahak,I.; Peretz,J.
Israel Journal of Chemistry, 1971 , vol. 9, p. 35 - 44
反应条件
N-butylamine in diethyl ether
参考文献
Tromelin, Anne; El Manouni, Driss; Burgada, R.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 301 - 312
反应条件
diethylamine T=60°C; 1.5 h; Microwave irradiation;
参考文献
Gruen, Alajos; Molnar, Istvan Gabor; Bertok, Bela; Greiner, Istvan; Keglevich, Gyoergy
Heteroatom Chemistry, 2009 , vol. 20, # 6 p. 350 - 354
反应条件
water 1.) ether, room temperature, 24 h; 2.) THF, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Sekine, Mitsuo; Satoh, Masaki; Yamagata, Hikaru; Hata, Tsujiaki
Journal of Organic Chemistry, 1980 , vol. 45, p. 4162 - 4167
反应条件
1: aq. HCl / tetrahydrofuran 2: aq. Na2CO3 3: HCl / diethyl ether View Scheme
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 18 p. 4811 - 4812
反应条件
1: 98 percent / NaI / acetone / 12 h / Ambient temperature 2: 95 percent / conc. aq. hydrochloric acid View Scheme
参考文献
Karaman, Rafik; Goldblum, Amiram; Breuer, Eli; Leader, Haim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 765 - 774
反应条件
(i) EtMgBr, Et2O, (ii) /BRN= 2050004/; Multistep reaction;
参考文献
Shahak,I.; Peretz,J.
Israel Journal of Chemistry, 1971 , vol. 9, p. 35 - 44
反应条件
water
1.) ether, room temperature, 24 h; 2.) THF, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Sekine, Mitsuo; Satoh, Masaki; Yamagata, Hikaru; Hata, Tsujiaki
Journal of Organic Chemistry, 1980 , vol. 45, p. 4162 - 4167
反应条件
in diethyl ether
0.05 h; Ambient temperature;
参考文献
Sekine, Mitsuo; Satoh, Masaki; Yamagata, Hikaru; Hata, Tsujiaki
Journal of Organic Chemistry, 1980 , vol. 45, p. 4162 - 4167
反应条件
water
1.) ether, room temperature, 24 h; 2.) THF, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Sekine, Mitsuo; Satoh, Masaki; Yamagata, Hikaru; Hata, Tsujiaki
Journal of Organic Chemistry, 1980 , vol. 45, p. 4162 - 4167
