1: Z-N-acetyl-a-aminocinnamic acid With hydrogen; [Rh(nbd)((Me3CCH2CMe2P(Me)CH2)2)]BF4 in methanol T=20°C; Catalytic hydrogenation; P=1520 Torr; 2 h; 2: diazomethyl-trimethyl-silane Esterification; Title compound not separated from byproducts;
参考文献
Sugiya, Masashi; Nohira, Hiroyuki
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 3 p. 705 - 712
in hexane Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Adger, Brian; Berens, Ulrich; Griffiths, Matthew J.; Kelly, Michael J.; McCague, Ray; Miller, John A.; Palmer, Christopher F.; Roberts, Stanley M.; Selke, Ruediger; Vitinius, Ute; Ward, Guy
Chemical Communications, 1997 , # 18 p. 1713 - 1714