1: diethylzinc; dihydro-3-(2-octen-1-yl)-2,5-furandione With [2,2']bipyridinyl; bis(acetylacetonate)nickel(II) in tetrahydrofuran
T=0°C; 3 h;
2: diazomethyl-trimethyl-silane With methanol in diethyl ether; benzene
T=20°C;
3: With hydrogen
Further stages. Title compound not separated from byproducts.;
参考文献
Rogers, Rebecca L.; Moore, Jennifer L.; Rovis, Tomislav
Angewandte Chemie - International Edition, 2007 , vol. 46, # 48 p. 9301 - 9304
1: methyl (S)-2-tert-butyloxycarbonylamino-3-phenylpropanoate With Dess-Martin periodane in dichloromethane
2: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in water; tert-butyl alcohol
3: diazomethyl-trimethyl-silane in methanol; toluene
参考文献
Harvey, Joanne E.; Kenworthy, Martin N.; Taylor, Richard J. K.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2467 - 2471