(1-氨基-甲基苯)磷酸合成路线 （共 34 条）
反应条件
1: With isobutyraldehyde,benzyl carbamate; acetic acid; phosphorus trichoride T=20°C; 2.33333 h; Heating / reflux; 2: With hydrogenchloride; water Heating / reflux; 3: With methyloxirane in methanol T=4 - 10°C;
参考文献
US2009/48426 A1, ;
Page/Page column 6 ;
反应条件
methyloxirane in ethanol
参考文献
Tetrahedron Letters, , vol. 37, # 3 p. 407 - 410
反应条件
1: With trimethylsilyl bromide; phosphorous acid trimethyl ester in toluene T=110°C; 3 h; 2: With methanol in dichloromethane 24 h;
参考文献
Polish Journal of Chemistry, , vol. 76, # 8 p. 1105 - 1111
反应条件
1: With hydrogenchloride in water; acetic acid 1 h; Reflux; 2: With hydrogen bromide in acetic acid T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 52, # 24 p. 3141 - 3145
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol; water 72 h;
参考文献
Liebigs Annalen der Chemie, , # 9 p. 955 - 958
反应条件
1: hydroxylamine hydrochloride / pyridine; methanol 2: 92 percent / MoO3, NaBH4 / methanol / 6 h / Ambient temperature 3: 96 percent / propylene oxide / ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 3 p. 407 - 410
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Tetrahedron Letters, , p. 677 - 680
反应条件
1: 50 percent / H2 / Pd/C(10percent) / acetic acid / 48 h / Ambient temperature 2: 65 percent / HCl aq. / acetic acid / 8 h / Heating View Scheme
参考文献
Synthesis, , # 12 p. 1028 - 1032
反应条件
1: (i) HPO(OEt)2, (ii) aq. HCl 2: H2 / Pd-C / acetic acid View Scheme
参考文献
Tetrahedron Letters, , p. 677 - 680
反应条件
1: acetic anhydride With orthophosphorus acid T=0 - 20°C; 2: N-benzylidene-α,α-diphenylbenzylamine T=0°C; 3: With hydrogenchloride; water 8 h; Reflux;
参考文献
Arkivoc, , vol. 2010, # 11 p. 360 - 369
