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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
18114-68-6
合成路线
（共 8 条）
578-57-4
2-溴苯甲醚
+
18114-68-6
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 6 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
577-19-5
1-溴-2-硝基苯
+
18114-68-6
→
反应条件
86-00-0
2-硝基联苯
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 6 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
88-73-3
邻氯硝基苯
+
18114-68-6
→
反应条件
86-00-0
2-硝基联苯
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 6 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
623-03-0
对氯苯甲腈
+
18114-68-6
→
反应条件
2920-38-9
4-氰基联苯
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 3 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
13329-40-3
4-碘代苯乙酮
+
18114-68-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol T=80°C; Suzuki-Miyaura reaction; 16 h;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
99-91-2
对氯苯乙酮
+
18114-68-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 6 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
99-90-1
4-溴苯乙酮
+
18114-68-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 3 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
104-92-7
4-溴苯甲醚
+
18114-68-6
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in 2-methoxy-ethanol Suzuki-Miyaura reaction; 4 h; Heating;
参考文献
Ito, Takatoshi; Iwai, Toshiyuki; Mizuno, Takumi; Ishino, Yoshio
Synlett, 2003 , # 10 p. 1435 - 1438
