(R)-N-环氧丙基邻苯二甲酰亚胺合成路线 （共 8 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20 - 25°C; 18 h;
参考文献
Gutcait, Alexander; Wang, Kuang-Chao; Liu, Hsiu-Wen; Chern, Ji-Wang
Tetrahedron Asymmetry, 1996 , vol. 7, # 6 p. 1641 - 1648
反应条件
potassium tert-butylate in isopropyl alcohol T=15°C; 4 h;
参考文献
DAISO CO., LTD.
Patent: EP1403267 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
1: With N-benzyl-N,N,N-trimethyl-ammonium chloride in isopropyl alcohol T=40°C; 24 h; 2: With potassium tert-butylate in isopropyl alcohol T=20°C; 3 h;
参考文献
Miki, Yasushi; Mikami, Masafumi
Patent: US2006/19993 A1, 2006 ;
Location in patent: Page/Page column 5 ;
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in tert-butyl alcohol T=20°C; 24 h;
参考文献
DAISO CO., LTD.
Patent: EP1403267 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride in DMF (N,N-dimethyl-formamide) T=20°C; 16 h;
参考文献
EP1403267 A1, ;
Page 6 ;
反应条件
sodium hydride in tetrahydrofuran 18 h; Product distribution / selectivity;
参考文献
KANEKA CORPORATION
Patent: EP1553093 A1, 2005 ;
Location in patent: Page/Page column 24 ;
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride; sodium carbonate in tert-butyl alcohol T=20°C; 23 h;
参考文献
DAISO CO., LTD.
Patent: EP1403267 A1, 2004 ;
Location in patent: Page 6-7 ;
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran 3 h; Inert atmosphereReflux; stereospecific reaction;
参考文献
Green Chemistry, , vol. 12, # 8 p. 1380 - 1382
