in toluene reaction in evacuated ampul; addn. of (Et3Ge)2Hg (in toluene) to toluenic soln. Co-compound; within 10 min soln. becomes light orange; pptn. of Hg;; removal of volatile byproducts (e.g. Et3GeCl) and solvent (vac.); low temp. crystn. in hexane;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 2370 - 2372,2197 - 2199
