2-乙基-1,1'-联苯合成路线 （共 20 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in diethyl ether; toluene T=80°C; 10 h;
参考文献
Guan, Bing-Tao; Xiang, Shi-Kai; Wang, Bi-Qin; Sun, Zuo-Peng; Wang, Yang; Zhao, Ke-Qing; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 11 p. 3268 - 3269
反应条件
copper (II) chromite T=200°C; P=102971 Torr; Hydrogenolyse;
参考文献
Huber et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1109,1111
反应条件
C43H54N2S; palladium diacetate; potassium carbonate in water; isopropyl alcohol T=100°C; Suzuki-Miyaura coupling reaction; 7 h; Aerobic conditionSealed tube;
参考文献
Li, Hong-Ling; Wu, Zhi-Sheng; Yang, Min; Qi, Yan-Xing
Catalysis Letters, 2010 , vol. 137, # 1-2 p. 69 - 73
反应条件
carbon dioxide; water; hydrogen; sulfur T=415°C; Molecular sieveHigh pressure; Reagent/catalystTemperature;
参考文献
Fan, Honglei; Wu, Tianbin; Yang, Guanying; Zhang, Peng; Ding, Guodong; Wang, Weitao; Jiang, Tao; Han, Buxing
Catalysis Communications, 2013 , vol. 33, p. 42 - 46
反应条件
iodine 1.) THF, RT, 2.) a) -78 deg C, 3 h, b) RT, 3 h; Yield given. Multistep reaction;
参考文献
Rieke, Reuben D.; Schulte, Louis D.; Dawson, Bryan T.; Yang, Sheng Sbeng
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8388 - 8398
反应条件
1: diethyl ether 2: copper chromite / 200 °C / 102971 Torr / Hydrogenolyse View Scheme
参考文献
Huber et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1109,1111
参考文献
Goodman; Wise
Journal of the American Chemical Society, 1950 , vol. 72, p. 3076,3077
反应条件
[VO(OEt)Cl2] 1.) Et2O, RT, 1 h, 2.) Et2O, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Ishikawa; Ogawa; Hirao
Journal of the American Chemical Society, 1998 , vol. 120, # 20 p. 5124 - 5125
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 72 percent; Overall yield = 32.8 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
aluminum oxide; bis(acetylacetonate)nickel(II) in toluene T=150°C; 12 h; Further byproducts given;
参考文献
Dzhemilev, U. M.; Kunakova, R. V.; Baibulatova, N. Z.; Tarasenko, A. E.; Mustafina, E. M.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 1 p. 160 - 166,128 - 134
