1,3-二(3-氯丙基)-1,1,3,3-四甲基二硅氧烷合成路线 （共 8 条）
反应条件
water in diethyl ether a) 0 deg C, b) RT, 1 h;
参考文献
Lafay, Jean; Latxague, Laurent; Lacroix, Christine; Deleris, Gerard
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 155 - 168
反应条件
1: With sodium hydroxide in methanol; water T=20°C; 1.5 h; 2: With potassium dihydrogenphosphate T=20°C; pH=7;
参考文献
JP2004/520272 A, ;
Page/Page column 14-15 ;
反应条件
trifluoro-methanesulfonic acid amide; triethylamine in tetrahydrofuran 13 h; Inert atmosphereReflux; Reagent/catalyst;
参考文献
Suslova; Albanov; Shainyan
Russian Journal of General Chemistry, 2013 , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., 2013 , vol. 83, # 3 p. 399 - 407,9
参考文献
Journal of the American Chemical Society, , vol. 82, p. 3601 - 3604
反应条件
triethylamine in methanol Reflux;
参考文献
Russian Journal of General Chemistry, , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., , vol. 83, # 3 p. 399 - 407,9
反应条件
1: dibenzoyl peroxide; hydrogen bromide / hexane / 6 h / |Inert atmosphere; |UV-irradiation 2: trifluoro-methanesulfonic acid amide; triethylamine / tetrahydrofuran / 13 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., , vol. 83, # 3 p. 399 - 407,9
反应条件
1: dibenzoyl peroxide; hydrogen bromide / hexane / 6 h / |Inert atmosphere; |UV-irradiation 2: triethylamine / methanol / |Reflux View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 83, # 3 p. 453 - 461
Zh. Obshch. Khim., , vol. 83, # 3 p. 399 - 407,9
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
