反应条件
thionyl chloride
byproducts: SO2; ratio of (CH3)2SbOSi(CH3)3 and SOCl2 1:2, freezing with liq. air, then warming up; seprd. by fractionation;
参考文献
Schmidbaur, H.; Arnold, H. S.; Beinhofer, E.
Chemische Berichte, 1964 , vol. 97, p. 449 - 458
Full Text Show Details
Gmelin Handbook: Sb: Org.Comp.2, 1.2.1.1.9.6, page 34 - 35
