氯(二甲基)2-噻吩基硅烷合成路线 （共 11 条）
反应条件
sulfuryl dichloride in dichloromethane T=20°C; Chlorination; 1 h;
参考文献
Gotteland; Junquero; Oms; Delhon; Halazy
Medicinal Chemistry Research, 1996 , vol. 6, # 5 p. 333 - 342
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperatureelectrochemical reduction;
参考文献
Moreau, Carole; Serein-Spirau, Francoise; Bordeau, Michel; Biran, Claude; Dunogues, Jacques
Journal of Organometallic Chemistry, 1996 , vol. 522, # 2 p. 213 - 221
反应条件
tetrabutylammomium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperatureelectrochemical reduction;
参考文献
Moreau, Carole; Serein-Spirau, Francoise; Bordeau, Michel; Biran, Claude; Dunogues, Jacques
Journal of Organometallic Chemistry, 1996 , vol. 522, # 2 p. 213 - 221
参考文献
Gmelin Handbook: Si: MVol.C, 61, page 173 - 175
反应条件
dihydrogen hexachloroplatinate; 3-(chloro)-prop-1-yne T=50°C; 6 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Lukevits, E.; Pudova, O. A.; Sturkovich, R. Ya.; Gaukhman, A. P.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 7 p. 1520 - 1523,1352 - 1354
反应条件
dihydrogen hexachloroplatinate T=50°C; 6 h; Product distribution;
参考文献
Lukevits, E.; Pudova, O. A.; Sturkovich, R. Ya.; Gaukhman, A. P.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 7 p. 1520 - 1523,1352 - 1354
反应条件
n-butyllithium 1.) THF, 0 deg C, 30 min, 2.) room temperature; Yield given. Multistep reaction;
参考文献
Zhang, Jian Xin; Dubois, Philippe; Jerome, Robert
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 6 p. 1209 - 1216
反应条件
dihydrogen hexachloroplatinate T=50°C; 6 h; Product distribution;
参考文献
Lukevits, E.; Pudova, O. A.; Sturkovich, R. Ya.; Gaukhman, A. P.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 7 p. 1520 - 1523,1352 - 1354
反应条件
tetrabutyl ammonium fluoride; copper(l) iodide in tetrahydrofuran; acetonitrile 0.0833333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Kim, Tae-Hyun; Pyun, Sung-Jae
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 6 p. 797 - 798
反应条件
diethyl ether; water
参考文献
Gen. Electric Co.
Patent: US2640818 , 1949 ;
