1,1,1,2,2-五氟丙烷合成路线 (共 55 条)
反应条件
hydrogen fluoride; tantalum pentafluoride T=149 - 150°C; 8 h; Product distribution / selectivity;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0108 ;
反应条件
hydrogen fluoride; catalyst (fluorine content: about 16.4 wt.percent) obtained by fluorinating a chromium oxide represented by the composition formula CrO2.0 T=281°C; P=750.075 Torr; 2 h; Inert atmosphere; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; YAMASHITA, Tsuneo; SUGIYAMA, Akinari
Patent: WO2010/101198 A1, 2010 ;
Location in patent: Page/Page column 15-16 ;
反应条件
hydrogen fluoride; chlorine T=350°C; Inert atmosphere; Temperature;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0104; 0105 ;
反应条件
hydrogen fluoride T=100 - 120°C; P=16274.9 Torr; 5 h; Product distribution / selectivity;
参考文献
ARKEMA INC.
Patent: WO2009/3084 A1, 2008 ;
Location in patent: Page/Page column 4-5 ;
反应条件
T=300°C; P=2250.23 Torr; 550 h; Gas phase; Product distribution / selectivity;
参考文献
ARKEMA FRANCE; DEUR-BERT, Dominique; PIGAMO, Anne; DOUCET, Nicolas; WENDLINGER, Laurent
Patent: WO2012/98420 A1, 2012 ;
Location in patent: Page/Page column 14-15 ;
反应条件
tri-n-butyl-tin hydride 2 h; Heating;
参考文献
Puy, Michael Van Der; Belter, Randolph K.; Borowski, Ralph J.; Ellis, Lois A. S.; Persichini, Phillip J.; et al.
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 59 - 64
反应条件
T=500°C; Inert atmosphere;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0117; 0118 ;
反应条件
hydrogen fluoride; 1percent Pd supported on fluorided alumina catalyst T=125 - 300°C; P=760.051 Torr; 0.00833333 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37742 A1, 2005 ;
Location in patent: Page/Page column 16; 19 ;
反应条件
T=575°C; 3 h; Inert atmosphere;
参考文献
E. I. du Pont de Nemours and Company; Mahler, Barry Asher; Nappa, Mario Joseph
Patent: EP2634165 A2, 2013 ;
Location in patent: Paragraph 0119; 0120 ;
反应条件
hydrogen fluoride; 2percentCo2O3/Cr2O3, fluorided T=275°C; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54781 A1, 2008 ;
Location in patent: Page/Page column 18-19 ;