氯甲基(二甲基)甲氧基硅烷合成路线 （共 14 条）
反应条件
triethylamine in pentane 1.) 0 deg C to rt, 2.) reflux, 4 h;
参考文献
Tacke, Reinhold; Lopez-Mras, Angel; Sperlich, Joerg; Strohmnann, Carsten; Kuhs, Werner F.; et al.
Chemische Berichte, 1993 , vol. 126, # 4 p. 851 - 862
反应条件
hydrogenchloride in 1,4-dioxane T=25°C; 1 h; Rate constantEquilibrium constant;
参考文献
Kohlheim; Lange; Kelling
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 7 p. 660 - 662
反应条件
triethylamine T=20°C; Reflux;
参考文献
Suslova; Shainyan
Russian Journal of General Chemistry, 2011 , vol. 81, # 8 p. 1735 - 1737
反应条件
T=140°C; var. temp., other alkali metals alkoxides, chloromethyldimethylhalosilanes, and chloromethyldimethylmethoxysilane; Product distributionMechanism;
参考文献
Hopper, Steven P.; Tremelling, Michael J.; Goldman, Emma W.
Journal of Organometallic Chemistry, 1980 , vol. 190, # 3 p. 247 - 256
反应条件
T=100°C; P=750.075 Torr; 4 h; Neat (no solvent);
参考文献
Schafer, Oliver; Bauer, Andreas; Kneissl, Andrea
Patent: US2006/122413 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogenchloride in 1,4-dioxane T=25°C; 1 h; Equilibrium constant;
参考文献
Kohlheim; Lange; Kelling
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 7 p. 660 - 662
反应条件
tetramethyl-ammonium iodide in N,N-dimethyl-formamide T=20 - 130°C; 3 h; Product distribution / selectivity;
参考文献
CONSORTIUM FUeR ELEKTROCHEMISCHE INDUSTRIE GMBH
Patent: WO2006/92324 A1, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
in benzene
byproducts: Et3GeCl; Irradiation (UV/VIS); Ge-compd. addn. to Si-compd. soln., sealing in evac. ampul, irradiation (DRT-375 quartz mercury lamp) until orange color of Ge-compd. disappeared (3 min); fractionation; elem. anal.;
参考文献
Rybin, L. I.; Vyazankina, O. A.; Vayzankin, N. S.; Gendin, D. V.; Leshina, T. V.; et al.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1807 - 1812
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 2025 - 2031
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1974 , vol. 44, # 7 p. 1496 - 1501,1468 - 1472
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1974 , vol. 44, # 7 p. 1496 - 1501,1468 - 1472
